摘要
A series of benzimidazoles containing furyl and aryl substituents at C-2 position have been synthesiszed by the reaction of 1,2,-phenylenediamine with corresponding carboxylic acids under microwave irradiation without solvent,in which artificial zeolite and catalytic amounts of DMF were used as the catalyst and the energy transfer medium,respectively. With such microwave techniques,the reaction times are remarkably shorted and the products are obtained in higher yields and cleaner reactions with easier workup than compared to conventional heating methods.
A series of benzimidazoles containing furyl and aryl substituents at C-2 position have been synthesiszed by the reaction of 1,2 ,-phenylenediamine with corresponding carboxylic acids under microwave irradiation without solvent , in which artificial zeolite and catalytic amounts of DMF were used as the catalyst and the energy transfer medium, respectively. With such microwave techniques, the reaction times are remarkably shorted and the products are obtained in higher yields and cleaner reactions with easier workup than compared to conventional heating methods.
出处
《四川大学学报（自然科学版）》
CAS
CSCD
北大核心
2005年第5期1054-1056,共3页
Journal of Sichuan University(Natural Science Edition)
基金
国家自然科学基金资助(20272038)
