摘要
[目的]开发一种缩短灭菌乳中糠氨酸含量检测时间的方法,可以提升乳制品质量控制效率。[方法]利用中红外光谱技术结合偏最小二乘法(PLS),定量分析样品中的糠氨酸含量,实现微量糠氨酸的快速简便定量检测。[结果]与农业行业标准方法《NY/T 939-2016巴氏杀菌乳和UHT灭菌乳中复原乳的鉴定》相比,本文糠氨酸定量检测方法结果出具时间由2天缩短至15 min。[结论]该方法重复性较好,精密度和准确性较高,符合检测要求,具有较好应用前景。
[Objective]To develop a method to shorten the detection time of furosine content in the sterile milk,so as to improve the quality control efficiency of dairy products.[Method]This paper used mid-infrared spectroscopy technology combined with partial least squares method(PLS)to quantitatively analyze the content of furosine in samples,and realized the rapid and simple quantitative detection of trace furosine.[Result]This method is compared with the agricultural industry standard method NY/T 939—2016:Identification of Reconstituted Milk in Pasteurized Milk and UHT Pasteurized Milk,the quantitative detection method for furosine developed in this paper reduced the time of results from 2 days to 15 minutes.[Conclusion]The method has good repeatability,high precision and accuracy,meets the detection requirements,and has a good application prospect.
作者
田桂艳
李慧
白晓玲
曹文燕
王丹慧
马建军
刘伯扬
李海军
逯刚
TIAN Guiyan;LI Hui;BAI Xiaoling;CAO Wenyan;WANG Danhui;MA Jianjun;LIU Boyang;LI HaiJun;LU Gang(Mengniu Dairy(Baoding)Co.,Ltd.,Baoding Hebei 072450)
出处
《中国乳业》
2023年第4期82-86,共5页
China Dairy
基金
呼和浩特市科技计划项目(重大科技专项)-乳制品食品安全风险识别及品质控制技术研究(2021-农-重-1)。
关键词
糠氨酸
中红外光谱技术
偏最小二乘法
复原乳的鉴定
furosine
mid-infrared spectroscopy
partial least square method
identification of recovered milk
