摘要
建立了从生产大豆异黄酮的废水中分离纯化较高浓度大豆皂苷B组分的方法。利用D101大孔树脂分离,研究不同分离纯化工艺参数对B组分大豆皂苷分离效果的影响,从而建立大豆皂苷B组分的分离纯化工艺。通过D101树脂分离纯化,使得大豆皂苷B组分的质量分数由0.67%提升至18.96%。通过利用低浓度的乙醇进行结晶以获得纯度更高的大豆皂苷B组分,纯度可提高至35%。
The method for purifying high purity soybean saponin B from waste water of soybean isoflavone production was established.By using D101 macroporous resin,the effects of different separation and purification parameters on the separation effect of B-component soybean saponin were studied,so as to establish the separation and purification process of B-component soybean saponin.Through the separation and purification of D101 resin,the content of B component of soybean saponin was increased from 0.67%to 18.96%.The purity of soybean saponin B could be increased to 35%by crystallization with low concentration of ethano.
作者
易清清
孟拥军
常庆
梁冬雨
章雨婷
姜国伟
Yi Qingqing;Meng Yongjun;Chang Qing;Liang Dongyu;Zhang Yuting;Jiang Guowei(Clinical Research Center,Jiading District Central Hospital Affiliated Shanghai University of Medicine&Health Sciences,Shanghai 201800;Departments of Pharmacy,Jiading District Central Hospital Affiliated Shanghai University of Medicine&Health Sciences,Shanghai 201800;School of Pharmacy,Shanghai University of Medicine&Health Sciences,Shanghai 201318)
出处
《中国粮油学报》
EI
CAS
CSCD
北大核心
2020年第8期141-145,共5页
Journal of the Chinese Cereals and Oils Association
基金
上海健康医学院种子基金(SFP-18-20-16-007)。
关键词
大豆皂苷B
D101大孔树脂
分离纯化
soybean saponin B
D101 macroporous resin
separation and purification
