摘要
目的:建立颈康酊质量标准。方法:采用TLC法对颈康酊中的三七、苏木、路路通药材进行定性鉴别,用HPLC法对三七中的人参皂苷Rbl进行含量测定研究。结果:TLC法可鉴定出制剂中的三七、苏木、路路通;人参皂苷Rbl在0. 856～8. 560μg范围内线性关系良好(r=0. 999 9),平均回收率为100. 30%,RSD为2. 70%(n=6)。结论:本法准确、简便、重复性好,可用于颈康酊的质量控制。
Objective:To establish the quality standard for Jingkang tincture.Methods:An TLC was adopted to identify Panax notoginseng(Burkill)F.H.Chen ex C.H.,Caesalpinia sappan L.and Fructus Liquidambaris in Jingkang tincture.HPLC was adopted to determine the content of ginsnoside Rb1 in Jingkang tincture.Results:Panax notoginseng(Burkill)F.H.Chen ex C.H.,Caesalpinia sappan L.and Fructus Liquidambaris could be identified by TLC.The linear range of ginsenoside Rb1 was 0.856-8.560!g(r=0.999 9),and the average recovery was 100.30%with the RSD of 2.70%(n=6).Conclusion:The method is simple,accurate and reproducible,which can be used for the quality control of Jingkang tincture.
作者
蓝保强
何蔚
邓聿胤
饶伟源
Lan Baoqiang;He Wei;Deng Yuyin;Rao Weiyuan(Guangxi Academy of Traditional Medical and Pharmaceutical Sciences,Nanning 530022,China;Guangxi Key Laboratory of Traditional Chinese Medicine Quality Standard;Shenzhen Jatai Pharmaceutical Co.Ltd.)
出处
《中国药师》
CAS
2019年第1期188-190,共3页
China Pharmacist
基金
广西壮族自治区卫生和计划生育委员会中药壮瑶药制剂提升工程项目(编号:GZZJ16-11)
