摘要
目的：建立仙慈丹（XCD）的质量标准。方法：采用薄层色谱法进行定性鉴别,RP-HPLC法进行定量测定。结果：建立了半枝莲、三七、姜黄、苏木的薄层色谱鉴别方法,建立了野黄芩苷的测定方法,野黄芩苷的加样回收率为100.55%（RSD为1.54%,n=6）,线性范围为0.032~0.481μg（r=0.999 9）。结论：所建立的定性、定量方法简便、准确、重复性好,专属性强,可较全面地控制仙慈丹的质量。
Objective： To establish the quality standard for Xiancidan. Method： TLC was used to qualitatively differentiate the material medicines; and RP-HPLC was used to detect the content of scutellarin. Result： The TLC identification method for ScuteUaria barbara, Caesalpinia sappan, Curcuma longa and Panax notoginseng （ Burk. ） F. H. Chen in the preparation was established. The con- tent of scutellarin was linear within the range of 0.032-0. 481 ~g（ r = 0. 999 9）. The average recovery was 100.55%. Conclusion： The methods are easily operated with promising specificity and repeatability, and convenient, reliable and accurate in the quality con- trol of Xiancidan
出处
《中国药师》
CAS
2013年第11期1644-1647,共4页
China Pharmacist
基金
广东省科技计划项目(编号:2010B030700001)
