摘要
目的 :建立救急行军散 (薄荷脑、冰片、黄芩、雄黄、朱砂、苏铁蕨贯众、陈皮等 )的质量标准。方法 :通过TLC、GC对散剂中的黄芩、陈皮、苏铁蕨贯众、薄荷脑、冰片进行鉴别研究 ;同时采用GC测定散剂中的薄荷脑、冰片含量。结果 :TLC色谱中均能明显地检出黄芩、陈皮、苏铁蕨贯众药材 ,GC色谱中均能明显地检出薄荷脑、冰片 ,GC法测得薄荷脑、冰片的含量分别为 75 .6 9～ 78.5 1mg·g-1和 6 1.2 6～ 6 4 .14mg·g-1,平均加样回收率为 :薄荷脑 99.35 % (RSD为 0 .98% ) ,冰片99 .2 4 % (RSD为 1.0 5 % )。结论 :所建立的方法简便可行 ,重现性好 。
Objective: To establish the quality standard for Jiujixingjun Power(Mentholum, Borneolum Syntheticum, Radix Scutellariae, Realgar, Cinnabaris, Brainia Insignis, Pericarpium Citri Reticulatae, etc.). Methods: Radix Scutellariae, Pericarpium Citri Reticulatae, Brainia Insignis, Mentholum and Borneolum Syntheticum in this medicine were identified by TLC and GC. The contents of Mentholum and Borneolum Syntheticum were determined by GC. Results: Radix Scutellariae and Pericarpium Citri Reticulatae and Brainia Insignis could be identified by TLC. Mentholum and Borneolum Syntheticum could be identified by GC. Its content was in the range of 75.69～78.51mg·g -1 and 61.26～ 64.14 mg·g -1 , respectively. The average recovery of Mentholum was 99.35%( RSD =0.98%) and Borneolum Syntheticum was 99.24%( RSD =0.98%). Conclusion: The method established is simple, feasible and reproducible and can be used as the quality standards for Jiujixingjun Powder.
出处
《中成药》
CAS
CSCD
北大核心
2003年第11期874-877,共4页
Chinese Traditional Patent Medicine
