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HS-SPME-GC-MS联用分析中成药保济丸挥发性成分 被引量:1

Analysis of volatile components of the Chinese medicine Baoji pills by HS-SPME-GC-MS
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摘要 采用顶空固相微萃取(HS-SPME)及气相色谱-质谱联用技术(GC-MS)分析保济丸中的挥发性成分。结果表明,利用HS-SPME-GC-MS法从中成药保济丸中分析出29种挥发性成分,验证了其中15种成分,相对含量占保济丸总挥发性成分的46.47%,其中含量最高的为十二碳烷(12.63%),其次为茅苍术醇(6.79%)、百秋李醇(4.80%)、石竹烯(3.66%)等。 Volatile components in Baoji pills were analyzed by using headspace solid-phase microextraction(HS-SPME) and gas chromatography-mass spectrometry(GC-MS). Results showed that a total of 29 volatile components were analyzed by HSSPME-GC-MS method from Chinese patent medicine Baoji pills, 15 of which were identified by experiments. The relative content accounts for 46.47% of the total volatile components of Baoji pills. The highest content was dodecane(12.63%), followed by atractylodes ethanol(6.79%), phenolic alcohol(4.80%) and caryophyllene(3.66%).
作者 骆宇燊 杨红兵 陈成 刘毅 卢金清 江汉美 李锦周 LUO Yu-shen;YANG Hong-bing;CHEN Cheng;LIU Yi;LU Jin-qing;JIANG Han-mei;LI Jin-zhou(Hubei University of Chinese Medicine,Wuhan 430065,China;Research and Development Center of Medicinal Plant in Hubei Province,Wuhan 430065,China)
出处 《湖北农业科学》 2019年第22期182-184,共3页 Hubei Agricultural Sciences
关键词 保济丸 挥发性成分 顶空固相微萃取 气质联用 Baoji pill volatile components HS-SPME GC-MS
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