摘要
目的:建立晕可平颗粒的质量标准。方法:采用薄层色谱法对晕可平颗粒中的夏枯草和车前草进行定性鉴别;采用高效液相色谱法测定咖啡酸和迷迭香酸的含量。结果:薄层色谱法能对夏枯草和车前草进行定性鉴别,斑点清晰,重复性好。咖啡酸测定的线性范围为0.007 12~0.142 4μg(r=0.999 8),平均回收率为97.78%(n=6);迷迭香酸测定的线性范围为0.063 9~1.278μg(r=0.9999),平均回收率为97.92%(n=6)。结论:该法简便、快速、准确,重现性好,可用于晕可平颗粒的质量控制。
Objective：To establish the quality standard for Yunkeping Granules. Methods： Prunellae spica and Plantaginis herba in Yunkeping Granules were identified by TLC; the content of Caffeic acid and Rosmarinic acid were determined by HPLC. Results： TLC can qualitative identification Prunellae spica and Plantaginis herba, spots were clear and repeatable. The linear range of determination of Caffeie acid in 0. 007 12~0. ld.2 4μg （r=0. 999 8）, the average recovery rate was 97.78% （n=6） ;the linear range of determination of Rosmarinie acid from 0. 0639~1. 278μg （r=0. 9999）, the average recovery rate was 97.92% （n=6）. Conclusion： The method is simple, rapid, accurate and reproducible. It can be used for quality control of Yunkeping Granules.
出处
《亚太传统医药》
2017年第20期40-42,共3页
Asia-Pacific Traditional Medicine
关键词
晕可平颗粒
质量标准
夏枯草
咖啡酸
迷迭香酸
Yunkeping Granules
Quality Standard
Prunellae Spica
Caffeic Acid
Rosmarinic Acid
