摘要
聚甲基丙烯酰亚胺(polymethacrylimide,PMI)泡沫复合材料具有众多优良特性,被广泛应用于航天航空、军工、船舶、汽车及高速列车等各个领域。而作为新型的夹层结构材料,其太赫兹(Terahertz,THz)波段的性能检测尚未见报道。基于THz时域光谱分析方法,对国内外两种型号的PMI泡沫复合材料在太赫兹波段透射及反射的实验获得的时域波形、功率密度谱进行了分析比较,基于MATALB编程、Origin8.0数据处理,应用时域、频域方法计算分析了不同厚度的德固赛(型号:Rohacell WF71)、美沃科技发展有限公司生产的(型号:SP1D80-P-30)PMI泡沫复合材料的透射率(传输函数)、吸收率、反射率以及折射率等光学参数。研究结果表明:通过对比空气、氮气中的不同测量结果,解释了湿度对测量结果的影响。PMI泡沫复合材料的折射率为1.05左右,功率谱的衰减是由于测试平台本身信号较弱、样品较厚且PMI泡沫的内部微结构的散射,造成THz波在>0.6THz波段表现出明显的衰减。该结论为THz波段在PMI泡沫复合材料方面的应用提供了理论依据,同时也为太赫兹无损探伤(non-destructive testing,NDT)技术在PMI泡沫复合材料方面的应用做了一个良好的铺垫。
Polymethaerylimide （PMI） foam composite has many excellent properties. Currently, PMI is heat-resistant foam, with the highest strength and stiffness. It is suitable as a high-performance sandwich structure core material. It can replace the honeycomb structure. It is widely used in aerospace, aviation, military, marine, automotive and high-speed trains, etc. But as new sandwich materials, PMI performance testing in the THz band is not yet visible. Based on the Terahertz （THz） time-domain spectroscopy technique, we conducted the transmission and reflection experiments, got the time domain waveforms and power density spectrum. And then we analyzed and compared the signals. The MATALB and Origin 8.0 was used to calculate and obtain the transmittance （transfer function）, absorptivity Coefficient, reflectance and the refractive index of the different thickness Degussa PMI （Model： Rohacell WF71）, which were based on the application of the time-domain and frequency-domain analysis methods. We used the data to compared with the THz refractive index and absorption spectra of a domestic PMI, Baod- ing Meiwo Technology Development Co. , Ltd. （Model： SPID80-P-30）. The result shows that the impact of humidity on the measurement results is obvious. The refractive index of PMI is about 1.05. The attenuation of power spectrum is due to the signal of the test platform is weak, the sample is thick and the internal scattering of PMI foam microstructure, This conclusion provides a theoretical basis for the THz band applications in the composite PMI. It also made a good groundwork for THz NDT （Non-Destructive Testing, NDT） technology in terms of PMI foam composites.
出处
《光谱学与光谱分析》
SCIE
EI
CAS
CSCD
北大核心
2015年第12期3319-3324,共6页
Spectroscopy and Spectral Analysis
基金
国家“十二五”科技支撑计划项目(2012BAK04B03)
重庆市应用开发重大项目(cstc2013yykfc00007)
中国科学院“西部之光”人才培养计划西部博士资助项目
国家教育部回国人员科研基金项目资助
