摘要
NiCo2O4 nanosheets with sheaf-like nanostructure morphologies have been synthesized by a facile one-step hydrothermal reaction followed by annealing treatment. Impressively, the NiCo2O4 nanosheets exhibit rapid detection of eugenol. The linear range of detection is from 1-500μM, and the limit of detection is 5.4 μM. The NiCo2O4 modified electrode demonstrated high sensitivity, good repeatability and reproducibility, and long-term stability （7% decrease in response over 30 days）. Based on this work, an electrochemical reaction mechanism for eugenol oxidation was proposed, and in addition, the NiCo2O4 modified electrode was successfully employed for the analysis of eugenol in medicative balm samples. Recovery values for eugenol in medicative balm samples were in the range 98.7%-105.5%.
NiCo <sub>2</sub > 有像捆的 nanostructure 形态学的 O <sub>4</sub> nanosheets 被热水的反应由退火跟随了的一出灵巧的一步舞综合了处理。给人深刻印象地， NiCo <sub>2</sub > O <sub>4</sub> nanosheets 展览 eugenol 的快速的察觉。察觉的线性范围从 1500 M，并且察觉的限制是 5.4 下午。NiCo <sub>2</sub > O <sub>4</sub> 修改了电极表明的高敏感，好重覆性和重制度，和长期的稳定性(在在 30 天的反应的 7% 减少) 。把工作基于这，为 eugenol 氧化的电气化学的反应机制被建议，并且另外， NiCo <sub>2</sub > O <sub>4</sub> 修改了电极成功地在药的香油样品为 eugenol 的分析被采用。为在药的香油样品的 eugenol 的恢复价值在范围 98.7%105.5% 。
