期刊文献+

紫外分光光度法测定泰乐菌素注射液含量方法的建立 被引量:8

Determination of Tylosin Injection Content by UV Spectrophotometry
在线阅读 下载PDF
导出
摘要 以0.1 mol/L盐酸溶液为参比液,采用紫外分光光度法在290 nm波长处测定泰乐菌素注射液中泰乐菌素的含量。结果表明,泰乐菌素在5 U/mL^50 U/mL浓度范围内,其吸光度与浓度呈良好的线性关系,相关系数r=0.999 2,平均回收率为99.6%,RSD为0.4(n=6)。该方法操作简便、快速、准确,适于作为生产企业中间产品的质量控制方法。 An UV spectrophotometry method for the determination of tylosin content in tylosin injection was established with 0. 1 mol/L hydrochloric acid as reference solution at 290 nm. The calibration curve for tylosin was linear within the concentration range of 5μg/mL-50 μg/mL(r= 0. 999 2). The average recovery rate was 99.6% ,and the RSD was 0.4%(n=6). This method was proved to be simple,rapid and precise, and can be used for the quality control of tylosin injection.
出处 《动物医学进展》 CSCD 北大核心 2009年第6期63-66,共4页 Progress In Veterinary Medicine
关键词 泰乐菌素 注射液 紫外分光光度法 含量测定 tylosin injection UV spectrophotometry content determination
  • 相关文献

参考文献11

二级参考文献37

  • 1王丽平,江善祥,史晓丽,万荣峰,郭永刚,冯秀娟.泰妙菌素的体外抑菌活性与一般毒性研究[J].畜牧与兽医,2004,36(6):4-6. 被引量:14
  • 2吕淑荣,何杰,杨磊,朗跃武.兽用抗菌新药替米考星的研究[J].动物科学与动物医学,2004,21(9):7-9. 被引量:11
  • 3周绪正,张继瑜,李剑勇,李宏胜,李金善,徐忠赞.替米考星对猪传染性胸膜肺炎的治疗试验[J].动物医学进展,2005,26(6):84-88. 被引量:19
  • 4韩文瑜.病原细菌检验技术[M].长春:吉林科技出版社,1992..
  • 5戴自英.临床抗菌药物学[M].北京:人民卫生出版社,1995.274.
  • 6B W 卡尔尼克.禽病学(第十版)[M].北京:中国农业出版社,1999.235-239.
  • 7Gatne M M, Badole P C, Somkuwar A P , et al. Pharmacokinetics of tiamulin in calves after single intramuscular administration[J]. Indian Vet J. 1994, 71: 1148-1149.
  • 8Gatne M M, Badole P C, Ranade V V. Pharmacokinetics of Tiamulin in sheep after single intramuscular administration[J]. Indian Vet J. 1995, 72: 287-289.
  • 9Markus J R, Sherma J, Method I V. Gas chromatographic determination of tiamulin residues in swine liver[J]. Journal of AOAC International. 1993, 76(2): 451-458.
  • 10Valcarcel L, Noa M. Determination of tiamulin in lung and meal of intoxicated pigs after the consuption of medicated feed[ J]. Revista-de-salud-Animal. 2000, 22(1): 59-60.

共引文献59

同被引文献90

引证文献8

二级引证文献53

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部