摘要
目的:研究国产狭叶番泻叶Cassia angustifolia Vahl的化学成分,积累对照品,以便系统比较国产与进口狭叶番泻叶内在质量的异同,更好的开发利用国产番泻叶。方法:利用溶剂提取法和各种色谱方法进行分离纯化,根据理化性质和光谱数据进行结构鉴定。结果:分离鉴定了6个化合物:胆甾醇(Cholesterol,Ⅰ),山柰酚-3-芸香糖苷(Kampferol-3-rutinoside,Ⅱ),1,6-二羟基-3-甲基-xanthone-8-羧酸(Calyxanthone,Ⅲ),3-甲氧基-4-羟基苯甲酸(3-methoxy-4-hydorxy-benzoic acid,Ⅳ),对二甲氨基苯甲醛(P-dimethylaminobenzaldehyde,Ⅴ),3,4-二羟基苯甲酸(3,4-dihydroxybenzoic acid,Ⅵ)。结论:6个化合物均为首次从该植物中分离得到。
Objective： To study the chemical constituents of the leaves of Cassia angustifolia Vahl. Methods ： Solvents extraction and various chromatographic methods were applied to separate and purify its constituents. The structures were elucidated on the basis of chemical evidence and spectral analysis. Results： Six compounds were obtained and identified as cholesterol（ Ⅰ ） ,kampferol-3-rutinoside （ Ⅱ ） , ealyxanthone （ Ⅲ ） , 3-methoxy-4-hydroxy-benzoie acid （ Ⅳ ） , p-dimethylaminobenzaldehyde （ Ⅴ ） , 3,4-dihydroxybenzoie acid （ Ⅵ ）. Conclusion： Six compounds（ Ⅰ -Ⅵ） are obtained from this plant for the first time.
出处
《中药材》
CAS
CSCD
北大核心
2007年第9期1082-1084,共3页
Journal of Chinese Medicinal Materials
基金
温州市科技局项目(G2004083)
