摘要
Poly(o-pheneylidiamine) was synthesized by using facial synthesis method.The FTIR spectra,UV-vis absorption spectra and X-ray diffraction patterns were used to characterize the molecular structures of the polymer.The morphologies of powders were studied by using TEM.Voltammetric study was done to investigate the electrochemical behaviors of poly(o-pheneylidiamine).The structure,crystallinity,morphology and electrochemical activity of the polymer were discussed.The results showed that Poly(o-pheneylidiamine) particles appeared as micro sticks in the micrograph,their diameter is from several decade nanometers to more than 100 nanometers.X-ray diffraction patterns showed the poly(o-pheneylidiamine) was highly ordered and put up a crystalloid form of suppositional simple cubic crystal.Voltammetric study indicated that the poly(o-pheneylidiamine) synthesized by facial synthesis method had good electrochemical activity.
Poly（o-pheneylidiamine） was synthesized by using facial synthesis method. The FTIR spectra, UV-vis absorption spectra and X-ray diffraction patterns were used to characterize the molecular structures of the polymer. The morphologies of powders were studied by using TEM. Voltammetric study was done to investigate the electrochemical behaviors of poly（o-pheneylidiamine）. The structure, crystallinity, morphology and electrochemical activity of the polymer were discussed. The results showed that Poly （o-pheneylidiamine） particles appeared as micro sticks in the micrograph, their diameter is from several decade nanometers to more than 100 nanometers. X-ray diffraction patterns showed the poly（o-pheneylidiamine） was highly ordered and put up a crystal- loid form of suppositional simple cubic crystal. Voltametric study indicated that the poly（o-pheneylidiamine） synthesized by facial synthesis method had good electrochemical activity.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2007年第4期409-412,共4页
Chemical Research and Application
基金
国家自然科学基金(20274035)资助项目
新疆大学青年启动基金(100096)资助项目
关键词
聚邻苯二胺
界面聚合
poly （o-pheneylidiamine）
facial Synthesis
