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高效液相色谱法测定固齿散中阿魏酸的含量 被引量:2

QUANTITATIVE ANALYSIS OF FERULIC ACID IN GU CHI SAN BY HPLC
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摘要 应用高效液相色谱法对中药固齿散中阿魏酸的含量进行了测定.样品采用超声波提取后,再转溶水中,乙醚萃取,最后以甲醇溶解并定容.本法可测定多种混合中药中的阿魏酸物含量,有效地排除药物中其它成分的干扰,方法简便、快速、准确,分离效果好.平均回收率96.2%,变异系数为2.1%. Determination of Ferulic acid's content in chinese medicine Gu Chi Sanby HPLC. The sampls were extracted by ultrasonic at first, then dissolved in waterand extracted by ether,at last dissolved in methanol and in constant volume. Themethod to determine Ferulic acid's content in several mixture chinese medicines.The interference of other components in the medicines was excluded efficiently.This was a simple, fast, accurate method and have a good separate effort. It's average recovery rate was 96. 2%, and Variation coefficient was 2. l%
出处 《华中师范大学学报(自然科学版)》 CAS CSCD 1995年第1期69-72,共4页 Journal of Central China Normal University:Natural Sciences
关键词 固齿散 阿魏酸 高效液相色谱 中药 含量 Gu Chi San ferulic acid ultrasonic extration high-pressure liquidchromatography
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参考文献2

  • 1尹钟洙,张凌云,徐理纳.当归及其成分阿魏酸对大鼠血小板聚集和5-HT释放的影响[J]药学学报,1980(06).
  • 2王宝〓.中成药质量标准与标准物质研究[M]中国医药科技出版社,1994.

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