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Effects of the extrusion parameters on microstructure,texture and room temperature mechanical properties of extruded Mg-2.49Nd-1.82Gd-0.2Zn-0.2Zr alloy
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作者 Chenjin Zhang Guangyu Yang +4 位作者 Lei Xiao Zhiyong Kan Jing Guo Qiang Li Wanqi Jie 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS 2025年第1期136-146,共11页
Microstructure,texture,and mechanical properties of the extruded Mg-2.49Nd-1.82Gd-0.2Zn-0.2Zr alloy were investigated at different extrusion temperatures(260 and 320℃),extrusion ratios(10:1,15:1,and 30:1),and extrusi... Microstructure,texture,and mechanical properties of the extruded Mg-2.49Nd-1.82Gd-0.2Zn-0.2Zr alloy were investigated at different extrusion temperatures(260 and 320℃),extrusion ratios(10:1,15:1,and 30:1),and extrusion speeds(3 and 6 mm/s).The experimental results exhibited that the grain sizes after extrusion were much finer than that of the homogenized alloy,and the second phase showed streamline distribution along the extrusion direction(ED).With extrusion temperature increased from 260 to 320℃,the microstructure,texture,and mechanical properties of alloys changed slightly.The dynamic recrystallization(DRX)degree and grain sizes enhanced as the extrusion ratio increased from 10:1 to 30:1,and the strength gradually decreased but elongation(EL)increased.With the extrusion speed increased from 3 to 6 mm/s,the grain sizes and DRX degree increased significantly,and the samples presented the typical<2111>-<1123>rare-earth(RE)textures.The alloy extruded at 260℃ with extrusion ratio of 10:1 and extrusion speed of 3 mm/s showed the tensile yield strength(TYS)of 213 MPa and EL of 30.6%.After quantitatively analyzing the contribution of strengthening mechanisms,it was found that the grain boundary strengthening and dislocation strengthening played major roles among strengthening contributions.These results provide some guidelines for enlarging the industrial application of extruded Mg-RE alloy. 展开更多
关键词 Mg-rare earth alloys extrusion temperature extrusion ratio extrusion speed strengthening mechanisms
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Grain morphology and plasticizing mechanism of AZ31 magnesium alloy curved profiles by staggered extrusion
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作者 CHEN Zi-yu LI Feng +2 位作者 LI Yuan-qi LI Chao SUN Lu 《Journal of Central South University》 2025年第2期319-331,共13页
Traditional manufacturing processes for lightweight curved profiles are often associated with lengthy procedures,high costs,low efficiency,and high energy consumption.In order to solve this problem,a new staggered ext... Traditional manufacturing processes for lightweight curved profiles are often associated with lengthy procedures,high costs,low efficiency,and high energy consumption.In order to solve this problem,a new staggered extrusion(SE)process was used to form the curved profile of AZ31 magnesium alloy in this paper.The study investigates the mapping relationship between the curvature,microstructure,and mechanical properties of the formed profiles by using different eccentricities of the die.Scanning electron microscopy(SEM)and electron backscatter diffraction techniques are employed to examine the effects of different eccentricity values(e)on grain morphology,recrystallization mechanisms,texture,and Schmid factors of the products.The results demonstrate that the staggered extrusion method promotes the deep refinement of grain size in the extruded products,with an average grain size of only 15%of the original billet,reaching 12.28μm.The tensile strength and elongation of the curved profiles after extrusion under the eccentricity value of 10 mm,20 mm and 30 mm are significantly higher than those of the billet,with the tensile strength is increased to 250,270,235 MPa,and the engineering strain elongation increased to 10.5%,12.1%,15.9%.This indicates that staggered extrusion enables curvature control of the profiles while improving their strength. 展开更多
关键词 staggered extrusion ECCENTRICITY curved profiles MICROSTRUCTURE mechanical properties
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Effect of extrusion ratio on microstructure and mechanical properties of AZ42 alloy sheet
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作者 Song-ke XIAO Xiao-jie ZHOU +5 位作者 Gang ZENG Hong-chao XIAO Xin-kai KANG Xian-zheng LU Xiao-min CHEN Jian ZHANG 《Transactions of Nonferrous Metals Society of China》 2025年第4期1109-1121,共13页
The microstructure and mechanical properties of Mg−4.5Al−2.5Zn−0.3Mn−0.2Ca(wt.%,designated as AZ42)alloys in extruded(at extrusion ratios of 28,20 and 11.5)and peak-aged states were investigated,by using optical micro... The microstructure and mechanical properties of Mg−4.5Al−2.5Zn−0.3Mn−0.2Ca(wt.%,designated as AZ42)alloys in extruded(at extrusion ratios of 28,20 and 11.5)and peak-aged states were investigated,by using optical microscopy,scanning electron microscopy,energy dispersive spectrometry and electron backscatter diffraction.The results show that extrusion produces a typical basal fiber texture and streamlines of second phases.All samples exhibit the lowest Schmid factor of basal slip(SFb)and the superior tensile yield strength(TYS)along extrusion direction(ED).The sample with extrusion ratio of 20 exhibits the largest average grain size,but the smallest SFb which compensates for the disadvantage of grain coarsening and maintains the strength.After being peak-aged at 175℃for 48 h,the sample with the extrusion ratio of 20 shows the optimal TYS along all the directions,compared to the other samples.This hopes to provide useful information for optimizing the deformation parameters of the AZ42 alloys. 展开更多
关键词 AZ42 alloy extrusion ratio Schmid factor STRENGTH aging-hardening
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Achieving Ultrahigh Strength in Mg-1.2Y-1.2Ni(at.%)Alloy via Tailoring Extrusion Rate
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作者 Xiaoqing Liu Xianke Zhang +8 位作者 Jinwei Gao Xiurong Zhu Lei Xiao Zhengchi Yang Lijun Tan Chubin Yang Biao Wu Huixin Chen Jiayu Huang 《Acta Metallurgica Sinica(English Letters)》 2025年第2期299-312,共14页
Mg-1.2Y-1.2Ni(at.%)alloy was extruded at 400℃with an extrusion ratio of 16:1 and different rates from 1 to 6 mm/s.The effect of extrusion rate on microstructure and mechanical properties of the Mg-1.2Y-1.2Ni alloy wa... Mg-1.2Y-1.2Ni(at.%)alloy was extruded at 400℃with an extrusion ratio of 16:1 and different rates from 1 to 6 mm/s.The effect of extrusion rate on microstructure and mechanical properties of the Mg-1.2Y-1.2Ni alloy was systematically investigated.With the increase of extrusion rate,the average recrystallized grain size of Mg-1.2Y-1.2Ni alloy and mean particle diameter of Mg2Ni phase were increased,while the density of geometrically necessary dislocation and the intensity of the basal texture were decreased.When extrusion rate increases from 1 to 6 mm/s,the tensile yield strength(TYS)of asextruded Mg-1.2Y-1.2Ni alloy decreases from 501 to 281 MPa,while the elongation to failure increases from 1.5%to 6.2%.The Mg-1.2Y-1.2Ni alloy extruded at 3 mm/s obtained TYS of 421 MPa,the ultimate tensile strength(UTS)of 440 MPa and elongation to failure of 2.6%,respectively,exhibiting comprehensive mechanical properties with relatively good plasticity and ultrahigh strength.The ultrahigh TYS of 501 and 421 MPa was mainly due to the strengthening from ultrafine recrystallized grains,high volume fraction long period stacking ordered(LPSO)phases and high density dislocations. 展开更多
关键词 Wrought Mg-Y-Ni alloy Ultrahigh strength Microstructure extrusion rate
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Improvement of strength and ductility of TC4_(p)/AZ91D magnesium matrix composites by modifying the extrusion ratio
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作者 Zuying Yu Kaihong Zheng +4 位作者 Xintao Li Jun Xu Jianxin Sun Nan Zhou Fusheng Pan 《Journal of Magnesium and Alloys》 2025年第2期746-759,共14页
In this study,AZ91D(Mg-9Al-Zn)alloys reinforced with 2 vol%TC4(Ti-6Al-4V)particles fabricated by semi-solid stir casting were extruded at different ratios,resulting in observed grain refinement effects.The research fi... In this study,AZ91D(Mg-9Al-Zn)alloys reinforced with 2 vol%TC4(Ti-6Al-4V)particles fabricated by semi-solid stir casting were extruded at different ratios,resulting in observed grain refinement effects.The research findings demonstrate that both TC4 andβ-Mg_(17)Al_(12) phases contribute to promoting dynamic recrystallization(DRX)nucleation.With increasing extrusion ratio,theβ-phase(Mg_(17)Al_(12))gradually fractures into smaller particles,leading to progressive grain refinement.Furthermore,the transition from〈01-10〉fiber texture to non-basal texture in theα-Mg matrix after hot extrusion is attributed to improved DRX behavior and activation of non-basal slip.As the extrusion ratio increases,the tensile strength and elongation(EL)of TC4_(p)/AZ91D composite improve significantly,reaching optimum comprehensive mechanical properties at an extrusion of 40:1 with a yield strength(YS)of 257 MPa,an ultimate tensile strength(UTS)of 357 MPa,and an EL of 9.7%.This remarkable strengthening effect is primarily attributed toβ-phase reinforcement,grain refinement strengthening,and strain hardening. 展开更多
关键词 Magnesium matrix composites Mechanical properties TC4 titanium alloy extrusion process
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Improving mechanical properties of extrusion additive manufacturing WC-9Co cemented carbide via green warm isostatic pressing
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作者 Cai CHEN Run-xing ZHOU +4 位作者 Zu-ming LIU Yong-xia LI Dan ZOU Yi-ming CHANG Xu-lin CHENG 《Transactions of Nonferrous Metals Society of China》 2025年第3期902-920,共19页
To tackle the common issue of green defects in material extrusion(MEX)additive manufacturing(AM)cemented carbides,warm isostatic pressing(WIP)was introduced to eliminate defects of MEX WC-9Co cemented carbide greens,t... To tackle the common issue of green defects in material extrusion(MEX)additive manufacturing(AM)cemented carbides,warm isostatic pressing(WIP)was introduced to eliminate defects of MEX WC-9Co cemented carbide greens,thereby improving both microstructure uniformity and mechanical properties of sintered bodies.The results indicate that WIP reduces defects in MEX greens,thus decreasing the dimensions and numbers of defects,modifying shapes of pores within sintered bodies,while preserving surface quality and shape characteristics.Compared with WC-9Co prepared via MEX followed by debinding and sintering(DS),the hardness of WC-9Co prepared using MEX-WIP-DS does not change significantly,ranging HV_(30)1494-1508,the transverse rupture strength increases by up to 49.3%,reaching 2998-3514 MPa,and the fracture toughness remains high,ranging 14.8-17.0 MPa·m^(1/2).The mechanical properties surpass comparable cemented carbides fabricated through other AM methods and are comparable to those produced by powder metallurgy.The integration of green WIP into MEX-DS broadens the MEX processing window,and improves the overall mechanical properties of MEX AM WC-Co cemented carbides. 展开更多
关键词 material extrusion additive manufacturing WC-Co cemented carbide warm isostatic pressing DEFECT microstructure mechanical properties
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Intricate interplay between shear stress and extrusion temperature in Mg−Al composite rods
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作者 Jian-xing ZHAO Chao-wei ZENG +4 位作者 Ting YUAN Wei PENG Zhen-wei SUN Ou ZHANG Hong-jun HU 《Transactions of Nonferrous Metals Society of China》 2025年第1期105-125,共21页
The Mg−Al composite rods of aluminum core-reinforced magnesium alloy were prepared by the extrusion−shear(ES)process,and the microstructure,deformation mechanism,and mechanical properties of the Mg−Al composite rods w... The Mg−Al composite rods of aluminum core-reinforced magnesium alloy were prepared by the extrusion−shear(ES)process,and the microstructure,deformation mechanism,and mechanical properties of the Mg−Al composite rods were investigated at different extrusion temperatures and shear stresses.The experimental results show that the proportion of dynamic recrystallization(DRX)and texture for Al and Mg alloys are controlled by the combination of temperature and shear stress.The texture type of the Al alloys exhibits slight variations at different temperatures.With the increase of temperature,the DRX behavior of Mg alloy shifts from discontinuous DRX(DDRX),continuous DRX(CDRX),and twin-induced DRX(TDRX)dominant to CDRX,the dislocation density in Mg alloy grains decreases significantly,and the average value of Schmid factor(SF)of the basalslip system increases.In particular,partial grains exhibit a distinct dominant slip system at 390℃.The hardness and thickness of the bonding layer,as well as the yield strength and elongation of the Mg alloy,reach their maximum at 360℃as a result of the intricate influence of the combined temperature and shear stress. 展开更多
关键词 Mg−Al composite rod texture evolution deformation mechanism intermetallic compound extrusion−shear process
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Predictive factors for coronal and sagittal graft extrusion length after using tendon autograft for medial meniscus reconstruction 被引量:1
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作者 Tian-Wang Zhu Xian-Xiang Xiang +2 位作者 Chun-Hui Li Rui-Xin Li Nan Zhang 《World Journal of Orthopedics》 2024年第11期1036-1046,共11页
BACKGROUND Meniscus extrusion occurs in most elderly individuals and most patients after meniscus allograft transplantation.The risk factors and correlative factors of meniscus extrusion have been extensively studied.... BACKGROUND Meniscus extrusion occurs in most elderly individuals and most patients after meniscus allograft transplantation.The risk factors and correlative factors of meniscus extrusion have been extensively studied.However,for using tendon autograft for meniscus reconstruction,both graft type and surgical method are different from those in previous studies on meniscus extrusion.AIM To identify predictive factors for coronal and sagittal graft extrusion length after using tendon autograft for medial meniscus reconstruction.METHODS Ten patients who underwent medial meniscus reconstruction with tendon autograft were selected for this retrospective observational study.The graft extrusions and potential factors were measured and correlation and regression analyses were performed to analyze their relationships.RESULTS The medial graft extrusion correlated with the preoperative bilateral hip-kneeankle angle difference,preoperative Kellgren-Lawrence grade,preoperative relative joint space width,and preoperative bilateral medial edge incline angle difference.The anterior graft correlated with the anterior tunnel edge distance at 1 week after operation.The posterior graft extrusion correlated with the preoperative bilateral hip-knee-ankle angle difference,preoperative relative joint space width,and posterior tunnel edge distance at 1 week after operation.The mean graft extrusion correlated with the preoperative bilateral hip-knee-ankle angle difference and preoperative relative joint space width.The preoperative joint space width and anterior and posterior tunnel edge distance at 1 week can be used to predict the medial,anterior,posterior,and mean graft extrusion length.CONCLUSION The preoperative joint space width and tunnel position can be used to predict the coronal and sagittal graft extrusion length after using tendon autograft for medial meniscus reconstruction. 展开更多
关键词 MENISCUS extrusion RECONSTRUCTION AUTOGRAFT GRAFT
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Improving the ductility and toughness of nano-TiC/AZ61 composite by optimizing bimodal grain microstructure via extrusion speed 被引量:1
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作者 Lingling Fan Mingyang Zhou +5 位作者 Wulve Lao Yuwenxi Zhang Hajo Dieringa Ying Zeng Yuanding Huang Gaofeng Quan 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2024年第8期3264-3280,共17页
In this study,the nano-TiC/AZ61 composites with different heterogeneous bimodal grain(HBG)structures and uniform structure are obtained by regulating the extrusion speed.The effect of HBG structure on the mechanical p... In this study,the nano-TiC/AZ61 composites with different heterogeneous bimodal grain(HBG)structures and uniform structure are obtained by regulating the extrusion speed.The effect of HBG structure on the mechanical properties of the composites is investigated.The increasing ductility and toughening mechanism of HBG magnesium matrix composites are carefully discussed.When the extrusion speed increases from 0.75 mm/s to 2.5 mm/s or 3.5 mm/s,the microstructure transforms from uniform to HBG structure.Compared with Uniform-0.75 mm/s composite,Heterogeneous-3.5 mm/s composite achieves a 116.7%increase in ductility in the plastic deformation stage and almost no reduction in ultimate tensile strength.This is mainly because the lower plastic deformation inhomogeneity and higher strain hardening due to hetero-deformation induced(HDI)hardening.Moreover,Heterogeneous-3.5 mm/s composite achieves a 108.3%increase in toughness compared with the Uniform-0.75 mm/s composite.It is mainly because coarse grain(CG)bands can capture and blunt cracks,thereby increasing the energy dissipation for crack propagation and improving toughness.In addition,the CG band of the Heterogeneous-3.5 mm/s composite with larger grain size and lower dislocation density is more conducive to obtaining higher strain hardening and superior blunting crack capability.Thus,the increased ductility and toughness of the Heterogeneous-3.5 mm/s composite is more significant than that Heterogeneous-2.5 mm/s composite. 展开更多
关键词 Nano-TiC/AZ61 composite extrusion speed Heterogeneous bimodal grain structure Increasing ductility mechanism Toughening mechanism
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Investigation of high rate mechanical flow followed by ignition for high-energy propellant under dynamic extrusion loading
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作者 Liying Dong Yanqing Wu +1 位作者 Kun Yang Xiao Hou 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第2期336-347,共12页
Investigating the ignition response of nitrate ester plasticized polyether(NEPE) propellant under dynamic extrusion loading is of great significant at least for two cases. Firstly, it helps to understand the mechanism... Investigating the ignition response of nitrate ester plasticized polyether(NEPE) propellant under dynamic extrusion loading is of great significant at least for two cases. Firstly, it helps to understand the mechanism and conditions of unwanted ignition inside charged propellant under accident stimulus.Secondly, evaluates the risk of a shell crevice in a solid rocket motor(SRM) under a falling or overturning scene. In the present study, an innovative visual crevice extrusion experiment is designed using a dropweight apparatus. The dynamic responses of NEPE propellant during extrusion loading, including compaction and compression, rapid shear flow into the crevice, stress concentration, and ignition reaction, have been firstly observed using a high-performance high-speed camera. The ignition reaction is observed in the triangular region of the NEPE propellant sample above the crevice when the drop weight velocity was 1.90 m/s. Based on the user material subroutine interface UMAT provided by finite element software LS-DYNA, a viscoelastic-plastic model and dual ignition criterion related to plastic shear dissipation are developed and applied to the local ignition response analysis under crevice extrusion conditions. The stress concentration occurs in the crevice location of the propellant sample, the shear stress is relatively large, the effective plastic work is relatively large, and the ignition reaction is easy to occur. When the sample thickness decreases from 5 mm to 2.5 mm, the shear stress increases from 22.3 MPa to 28.6 MPa, the critical value of effective plastic work required for ignition is shortened from 1280 μs to 730 μs, and the triangular area is easily triggering an ignition reaction. The propellant sample with a small thickness is more likely to stress concentration, resulting in large shear stress and effective work, triggering an ignition reaction. 展开更多
关键词 NEPE propellant Crevice extrusion Shear flow Sample thickness Ignition reaction
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Deformation mechanisms and microstructural characteristics of AZ61 magnesium alloys processed by a continuous expansion extrusion approach
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作者 Yang Mo Fulin Jiang +4 位作者 Hang Xu Jie Tang Dingfa Fu Hui Zhang Jie Teng 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2024年第7期2826-2846,共21页
The unique continuous extrusion-based severe plastic deformation approaches were proposed recently to process high-performance magnesium (Mg) alloys,while the in-depth deformation mechanisms under such complicated the... The unique continuous extrusion-based severe plastic deformation approaches were proposed recently to process high-performance magnesium (Mg) alloys,while the in-depth deformation mechanisms under such complicated thermomechanical conditions were not well understood In the present work,the fundamental deformation behaviors of AZ61 Mg alloy from 25 to 400°C were firstly examined under uniaxial compression deformation.Then the deformation mechanisms and microstructural characteristics of AZ61 Mg alloy during continuous expansion extrusion forming (CEEF) were systematically investigated by microstructural observations,finite element and cellular automata simulations The results showed that the continuous evolutions of temperature,larger strain level and complex stress state with strain rate range of 0~5.98 s-1during CEEF brought the distinctive dynamic recrystallization behaviors and texture development in AZ61 Mg alloy,which were different to that of uniaxial compression deformation.In details,a remarkable grain refinement was achieved via CEEF processing due to the simultaneous actions of continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX).Gradually enhanced CDRX were observed from center to edge region,which had significant effects on the texture distribution and texture strength.The c-axis of most grains rotated under distinctive shear strain following parabolic metal flow,resulting in stable fiber texture.In addition,the evolution of the internal texture of the alloy led to an obvious increase in the Schmid factor for the activation of basal(c+a)slip system.©2022 Chongqing University.Publishing services provided by Elsevier B.V.on behalf of Ke Ai Communications Co.Ltd. 展开更多
关键词 Magnesium alloy Deformation Continuous expansion extrusion forming Microstructure Finite element simulation
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Extrusion 3D printing of carbon nanotube-assembled carbon aerogel nanocomposites with high electrical conductivity
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作者 Lukai Wang Jing Men +4 位作者 Junzong Feng Yonggang Jiang Liangjun Li Yijie Hu Jian Feng 《Nano Materials Science》 EI CAS CSCD 2024年第3期312-319,共8页
Carbon nanotubes(CNTs)with high aspect ratio and excellent electrical conduction offer huge functional improvements for current carbon aerogels.However,there remains a major challenge for achieving the on-demand shapi... Carbon nanotubes(CNTs)with high aspect ratio and excellent electrical conduction offer huge functional improvements for current carbon aerogels.However,there remains a major challenge for achieving the on-demand shaping of carbon aerogels with tailored micro-nano structural textures and geometric features.Herein,a facile extrusion 3D printing strategy has been proposed for fabricating CNT-assembled carbon(CNT/C)aerogel nanocomposites through the extrusion printing of pseudoplastic carbomer-based inks,in which the stable dispersion of CNT nanofibers has been achieved relying on the high viscosity of carbomer microgels.After extrusion printing,the chemical solidification through polymerizing RF sols enables 3D-printed aerogel nanocomposites to display high shape fidelity in macroscopic geometries.Benefiting from the micro-nano scale assembly of CNT nanofiber networks and carbon nanoparticle networks in composite phases,3D-printed CNT/C aerogels exhibit enhanced mechanical strength(fracture strength,0.79 MPa)and typical porous structure characteristics,including low density(0.220 g cm^(-3)),high surface area(298.4 m^(2)g^(-1)),and concentrated pore diameter distribution(~32.8nm).More importantly,CNT nanofibers provide an efficient electron transport pathway,imparting 3D-printed CNT/C aerogel composites with a high electrical conductivity of 1.49 S cm^(-1).Our work would offer feasible guidelines for the design and fabrication of shape-dominated functional materials by additive manufacturing. 展开更多
关键词 Carbon aerogel extrusion 3D printing Carbon nanotube Electrical conductivity RHEOLOGY
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Modeling of recrystallization behaviour of AA6xxx aluminum alloy during extrusion process
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作者 Marco NEGOZIO Antonio SEGATORI +3 位作者 Riccardo PELACCIA Barbara REGGIANI Sara Di DONATO Lorenzo DONATI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2024年第10期3170-3184,共15页
An innovative approach was introduced for the development of a AA6063 recrystallization model.This method incorporated a regression-based technique for the determination of material constants and introduced novel equa... An innovative approach was introduced for the development of a AA6063 recrystallization model.This method incorporated a regression-based technique for the determination of material constants and introduced novel equations for assessing the grain size evolution.Calibration and validation of this methodology involved a combination of experimentally acquired microstructural data from the extrusion of three different AA6063 profiles and results from the simulation using the Qform Extrusion UK finite element code.The outcomes proved the agreement between experimental findings and numerical prediction of the microstructural evolution.The trend of the grain size variation based on different process parameters was accurately simulated,both after dynamic and static recrystallization,with an error of less than 25% in almost the whole sampling computations. 展开更多
关键词 recrystallization simulation aluminum alloy extrusion finite element method microstructure prediction
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Method of fabricating artificial rock specimens based on extrusion free forming(EFF)3D printing
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作者 Xiaomeng Shi Tingbang Deng +2 位作者 Sen Lin Chunjiang Zou Baoguo Liu 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2024年第4期1455-1466,共12页
Three-dimensional(3D)printing technology has been widely used to create artificial rock samples in rock mechanics.While 3D printing can create complex fractures,the material still lacks sufficient similarity to natura... Three-dimensional(3D)printing technology has been widely used to create artificial rock samples in rock mechanics.While 3D printing can create complex fractures,the material still lacks sufficient similarity to natural rock.Extrusion free forming(EFF)is a 3D printing technique that uses clay as the printing material and cures the specimens through high-temperature sintering.In this study,we attempted to use the EFF technology to fabricate artificial rock specimens.The results show the physico-mechanical properties of the specimens are significantly affected by the sintering temperature,while the nozzle diameter and layer thickness also have a certain impact.The specimens are primarily composed of SiO_(2),with mineral compositions similar to that of natural rocks.The density,uniaxial compressive strength(UCS),elastic modulus,and tensile strength of the printed specimens fall in the range of 1.65–2.54 g/cm3,16.46–50.49 MPa,2.17–13.35 GPa,and 0.82–17.18 MPa,respectively.It is capable of simulating different types of rocks,especially mudstone,sandstone,limestone,and gneiss.However,the simulation of hard rocks with UCS exceeding 50 MPa still requires validation. 展开更多
关键词 Artificial rock 3D printing extrusion free forming(EFF) Similarity analysis Mechanical properties
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Application of Extrusion Cooking to Enhancing Mineral Bioaccessibility in Millet Flour Enriched with Natural Fortificants for Vulnerable Populations
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作者 Maty Diop Cheikh Ndiaye +3 位作者 John Lubaale Abdoulaye Séne Mohamed Lamine Gaye Djibril Traoré 《Food and Nutrition Sciences》 2024年第12期1357-1380,共24页
Background: Minerals bioaccessibility of food products could be increased by enhancing the apparent absorption of most minerals with the reduction of anti-nutritional factors (phytates) through extrusion cooking. The ... Background: Minerals bioaccessibility of food products could be increased by enhancing the apparent absorption of most minerals with the reduction of anti-nutritional factors (phytates) through extrusion cooking. The aim of the study was to increase the mineral bioaccessibility in co-extruded millet flours enriched with Moringa and Baobab for vulnerable populations. Methods: Three extruded instant formulas were developed using pearl millet, Moringa and Baobab powders: FA (90% Millet + 10% Baobab);FB (90% Millet + 10% Moringa);FC (80% Millet + 10% Baobab + 10% Moringa). Non-extruded formulations of FA, FB and FC were used as controls. Then treatments and controls were analyzed to determine their percent mineral bioaccessibility using the in vitro equilibrium dialysability method (Miller et al., 1981) and their total amounts bioaccessible according to the Burgos et al., 2018 method. Phytates in all samples were also determined using the Method of Fruhbeck et al., 1995. Results: Extrusion cooking significantly improved iron bioaccessible percentages in co-extruded flours respectively in FB and FC (p . Extrusion significantly reduced the percentages and amounts of bioaccessible zinc and calcium in all extruded flours compared to their controls (p Conclusion: Extrusion cooking reduced the chelation effect of phytates by thermal degradation, which led to a modification in the bioavailability of minerals. Food-to-food fortification and extrusion cooking displayed a positive effect on the bioaccessibility of iron, magnesium and phosphorus. For calcium and zinc, extrusion has no positive effect on their bioaccessibilities. However, with daily consumption, co-extruded fortified flours could be used as a way to fight against malnutrition in vulnerable populations. 展开更多
关键词 Iron Zn Mg P CALCIUM extrusion BIOACCESSIBILITY Dialysability
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Achieving high strength-ductility synergy in Mg-6Sn-3Zn-0.3Zr(wt.%)alloy via a combination of casting,pre-treatment and hot extrusion
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作者 Tianshui Zhou Yaqin Li +3 位作者 Feifei Guo Qinglin Li Zhi Jia Dexue Liu 《Journal of Magnesium and Alloys》 CSCD 2024年第11期4622-4645,共24页
Achieving the strength-ductility synergy in Mg alloys is a gigantic challenge,especially in rare-earth-free Mg alloys.In this study,a new Mg-Sn-Zn-Zr alloy with high ultimate tensile strength(~284-326 MPa)without sacr... Achieving the strength-ductility synergy in Mg alloys is a gigantic challenge,especially in rare-earth-free Mg alloys.In this study,a new Mg-Sn-Zn-Zr alloy with high ultimate tensile strength(~284-326 MPa)without sacrificing elongation-to-failure(~22.1-27.6%)was developed by utilizing casting,pre-treatment and hot extrusion.Strong random rather than basal texture is observed both in as-cast and pre-treatment samples.Subsequently,the strong texture is effectively weakened via hot extrusion whilst remaining random.More importantly,after hot extrusion,the grain sizes of as-cast and pre-treatment samples were significantly refined down to about 10μm.Examination of as-extruded microstructures of the alloy reveals that the grain refinement is highly associated with the particle stimulated nucleation(PSN)and continuous/discontinuous dynamic recrystallization(C/DDRX)mechanisms.Moreover,the results suggest that the combination of pre-treatment and hot extrusion not only promotes multiplication of geometrically-necessary dislocations(GNDs)but enhances dynamic precipitation,which boosts the formation of fine and homogenous precipitates.Based on the results of X-ray diffraction(XRD),transmission electron microscope(TEM)and selected area electron diffraction(SAED),the precipitates are Mg_(2)Sn phases.Furthermore,the main orientation relationship identified by high resolution TEM(HRTEM)between Mg_(2)Sn phases andα-Mg matrix could be described as(111)Mg_(2)Snor(220)Mg_(2)Sn∥(0001)Mgwith a coherent interface.The refined grains size,ultra-fine precipitates and high density of GNDs would substantially contribute to the enhancement of the strength and the corresponding contributions are calculated to be~183-185 MPa,~30.9-38 MPa and~14.2-31.7 MPa,respectively.Besides,texture weakening or randomizing,grain refinement and coherent interfaces are mainly responsible for the high ductility.The current study can provide beneficial insights into the development of high-performance rare-earth-free Mg alloys with favorable microstructure via a combination of casting,pre-treatment and hot extrusion processing. 展开更多
关键词 Mg-Sn-Zn-Zr alloy Hot extrusion Pre-treatment Mechanical properties Microstructure evolution Strengthening and plasticity mechanisms
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Development of the rolling extrusion rock bolt with constant resistance and large deformation
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作者 Yundong Shou Limin Guo Xiaoping Zhou 《Deep Resources Engineering》 2024年第1期41-52,共12页
With the increasing excavation depth of underground engineering,engineering problems such as large deformation and rock burst caused by high geo-stress brings new challenges to the excavation and reinforcement of surr... With the increasing excavation depth of underground engineering,engineering problems such as large deformation and rock burst caused by high geo-stress brings new challenges to the excavation and reinforcement of surrounding rock in deep underground engineering.The traditional rock bolt is prone to brittle fracture under high geo-stress due to its low elongation.Therefore,this work aims to develop a novel energy-absorbing bolt with constant resistance and large displacement to reinforce the surrounding rock with a risk of large deformation or rockburst.The novel energy-absorbing bolt refereed as rolling extrusion rock bolt(RE bolt)is mainly consists of sleeve tube with a variable cross-section,energy absorption slider with steel balls embedded,steel bar connected with the energy absorption slider.The rolling extrusion is adopted to produce the resistance force of the RE bolt,which avoids the sudden attenuation of resistance force and the abrasion of the energy absorption slider.The static pull test is conducted to study the resistance force and deformation characteristics of the RE bolt with different specifications.Results imply that the RE bolt has higher resistance force,larger deformation capacity and energy absorption capacity.The work of this study provides an effective solution for the reinforcement of surrounding rock in deep rock engineering. 展开更多
关键词 Energy-absorbing bolt Rolling extrusion Static pull test Constant resistance Large deformation
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Extrusion force analysis of aluminum pipe fabricated by CASTEX using expansion combination die 被引量:3
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作者 曹富荣 温景林 +3 位作者 丁桦 王昭东 于传平 夏飞 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2014年第11期3621-3631,共11页
To determine the extrusion force of pipe fabricated by continuous casting and extrusion (CASTEX) using an expansion combination die, the metallic expansion combination die was divided into diversion zone, expansion zo... To determine the extrusion force of pipe fabricated by continuous casting and extrusion (CASTEX) using an expansion combination die, the metallic expansion combination die was divided into diversion zone, expansion zone, flow dividing zone, welding chamber, and sizing zone, and the corresponding stress formulae in various zones were established using the slab method. The deformation zones of CASTEX groove were divided into liquid and semisolid zone, solid primary gripping zone, and solid gripping zone, and the formulae of pipe extrusion forces were established. Experiments were carried out on the self-designed CASTEX machine to obtain the aluminum pipe and measure its extrusion force using the expansion combination die. The experimental results of radial extrusion force for aluminum pipe are in good agreement with the calculated ones. 展开更多
关键词 continuous casting and extrusion continuous extrusion expansion combination die aluminum pipe stress analysis extrusion force
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Effect of process parameters on sheath forming of continuous extrusion sheathing of aluminum 被引量:4
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作者 赵颖 宋宝韫 +3 位作者 运新兵 裴久杨 贾春博 阎志勇 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2012年第12期3073-3080,共8页
The effect of flow passage length in the die cavity and extrusion wheel velocity on the shape of aluminum sheath during the continuous extrusion sheathing process was analyzed by using finite element methods based on ... The effect of flow passage length in the die cavity and extrusion wheel velocity on the shape of aluminum sheath during the continuous extrusion sheathing process was analyzed by using finite element methods based on software DEFORM 3D and experimentally validated. The results show that by increasing the flow passage length, the velocity of metal at the cross-section of sheath tends toward uniformity, the values of the bending angles of sheath gradually approach the ideal value of zero and the cross-section exhibits a better shape. The extrusion wheel velocity has negligible effects on the bending shape and cross-section of the sheath product when a long flow passage is used. 展开更多
关键词 continuous extrusion sheathing aluminum sheath sheath forming die design extrusion wheel velocity finite element
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Force analysis and experimental study of pure aluminum and Al-5%Ti-1%B alloy continuous expansion extrusion forming process 被引量:9
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作者 曹富荣 温景林 +4 位作者 丁桦 王昭东 李英龙 管仁国 侯辉 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第1期201-207,共7页
The deformation zone of CONFORM extrusion was divided into primary gripping zone,gripping zone,conical expansion chamber zone,cylindrical zone and sizing zone of die,and corresponding force equilibrium equations were ... The deformation zone of CONFORM extrusion was divided into primary gripping zone,gripping zone,conical expansion chamber zone,cylindrical zone and sizing zone of die,and corresponding force equilibrium equations were established using the Slab method.The deformation force formulae of CONFORM machine at any wrapping angle with an expansion chamber were obtained.Experiment on pure aluminum and Al-5%Ti-1%B alloy was conducted on the CONFORM machine self-designed.The resistance to deformation of Al-5%Ti-1%B alloy at the deformation temperature of 400℃ and the strain rate of 3.07 s-1 was measured to be 50 MPa using Gleeble-1500 thermal simulation machine.The calculation results of deformation forces for CONFORM process with an expansion chamber for pure aluminum and Al-5%Ti-1%B alloy were given.The experimental CONFORM radial force is in agreement with the radial force obtained by theoretical formula. 展开更多
关键词 ALUMINUM aluminum alloy continuous extrusion expansion chamber resistance to deformation
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