为了研究等温锻造温度对机械外壳用Mg-8Al-1Zn-0.5Ca镁合金组织与性能的影响,选择5种等温锻造温度对合金试样进行锻造试验,并进行了显微组织分析、耐腐蚀和耐磨损性能的测试与分析。结果发现:随着等温锻造温度从340℃增加至420℃,Mg-8Al...为了研究等温锻造温度对机械外壳用Mg-8Al-1Zn-0.5Ca镁合金组织与性能的影响,选择5种等温锻造温度对合金试样进行锻造试验,并进行了显微组织分析、耐腐蚀和耐磨损性能的测试与分析。结果发现:随着等温锻造温度从340℃增加至420℃,Mg-8Al-1Zn-0.5Ca镁合金的平均晶粒尺寸先减小后增大、腐蚀电位先正移后负移、磨损体积先减小后增大,合金的耐腐蚀和耐磨损性能先变好后变差。相较于等温锻造温度为340℃,等温锻造温度为400℃时的Mg-8Al-1Zn-0.5Ca镁合金的平均晶粒尺寸减小了76.1%、腐蚀电位正移141 m V、磨损体积减小了66.2%。研究结果表明,Mg-8Al-1Zn-0.5Ca镁合金的等温锻造温度优选为400℃。展开更多
The effects of the ultrasonic treatment on the microstructure and mechanical properties of Mg-6Zn-0.5Y-2Sn alloy were investigated. The results show that the ultrasonic treatment has significant effect on the microstr...The effects of the ultrasonic treatment on the microstructure and mechanical properties of Mg-6Zn-0.5Y-2Sn alloy were investigated. The results show that the ultrasonic treatment has significant effect on the microstructure and mechanical properties of Mg-6Zn-0.5Y-2Sn alloy. The phases in Mg-6Zn-0.5Y-2Sn alloy are α-Mg, MgZn2, MgSnY, Mg2Sn, and a small amount of I-phase. With the application of ultrasonic treatment, I-phase nearly disappears, and with increasing the ultrasonic treatment power, the coarse dendrites gradually change into roundish equiaxed grains. The second phases at the α-Mg boundaries transform from coarse, semicontinuous and non-uniform to fine, discontinuous, uniform and dispersive. When the ultrasonic treatment power is 700 W, the best comprehensive mechanical properties of Mg-6Zn-0.5Y-2Sn alloy are obtained. Compared with the untreated alloy, the 0.2%tensile yield strength, ultimate tensile strength and elongation are improved by 28%, 30%and 67%, respectively.展开更多
In this work,a high-strength Mg–10Gd–6Y–1.5Zn–0.5Zr(wt.%)alloy was fabricated by successive multi-pass equal channel angular pressing(ECAP).The microstructure and mechanical property of as-cast and ECAP alloys wer...In this work,a high-strength Mg–10Gd–6Y–1.5Zn–0.5Zr(wt.%)alloy was fabricated by successive multi-pass equal channel angular pressing(ECAP).The microstructure and mechanical property of as-cast and ECAP alloys were systematically researched by X-ray diffractometer,scanning electron microscopy,transmission electron microscopy and compression test.The results show that the microstructure of as-cast alloy consists ofα-Mg grains,Mg24Y5 networks,18R blocks,fine 14H lamellas,and fewY-rich particles.After 8 passes ECAP,dynamic recrystallization ofα-Mg is developed and their average grain size decreases to about 1μm.The network Mg_(24)Y_(5) phase at grain boundaries is broken into small particles with average diameter lower than 0.5μm.Moreover,18R blocks are kinked and delaminated,or broken into small particles and blended with Mg24Y5 particles.14H lamellas grow gradually or are dynamically precipitated within certainα-Mg grains.Compression tests indicate that 8p ECAP alloy exhibits excellent mechanical property with compressive strength of 537 MPa and fracture strain of 17.0%.The significant improvement for both strength and ductility of deformed alloy could be ascribed to DRX grains,refined Mg24Y5 particles,18R kinking and dynamical precipitation of 14H.展开更多
Mg?1Zn?0.5Ca alloys were prepared by traditional steel mould casting and water-cooled copper mould injection casting at higher cooling rate. Microstructure, mechanical properties and bio-corrosion resistance of two al...Mg?1Zn?0.5Ca alloys were prepared by traditional steel mould casting and water-cooled copper mould injection casting at higher cooling rate. Microstructure, mechanical properties and bio-corrosion resistance of two alloys were contrastively investigated. Grain size reduces remarkably and microstructure becomes homogenous when raising cooling rate. The bio-corrosion behaviour in 3.5% sodium chloride solution (3.5% NaCl) and Hank’s solution at 37°C was investigated using electrochemical polarization measurement and the results indicate that the alloy prepared at higher cooling rates has better corrosion resistance in both types of solution. Further mass loss immersion test in Hank’s solution reveals the same result. The reason of corrosion resistance improvement is that raising cooling rate brings about homogeneous microstructure, which leads to micro-galvanic corrosion alleviation. The tensile test results show that yield strength, ultimate tensile strength and elongation are improved by raising cooling rate and the improvement is mainly due to grain refinement.展开更多
文摘为了研究等温锻造温度对机械外壳用Mg-8Al-1Zn-0.5Ca镁合金组织与性能的影响,选择5种等温锻造温度对合金试样进行锻造试验,并进行了显微组织分析、耐腐蚀和耐磨损性能的测试与分析。结果发现:随着等温锻造温度从340℃增加至420℃,Mg-8Al-1Zn-0.5Ca镁合金的平均晶粒尺寸先减小后增大、腐蚀电位先正移后负移、磨损体积先减小后增大,合金的耐腐蚀和耐磨损性能先变好后变差。相较于等温锻造温度为340℃,等温锻造温度为400℃时的Mg-8Al-1Zn-0.5Ca镁合金的平均晶粒尺寸减小了76.1%、腐蚀电位正移141 m V、磨损体积减小了66.2%。研究结果表明,Mg-8Al-1Zn-0.5Ca镁合金的等温锻造温度优选为400℃。
基金Project(cstc2015jcyj BX0036)supported by Chongqing Research Program of Basic Research and Frontier Technology,ChinaProject(51571040)supported by the National Natural Science Foundation of ChinaProject supported by the Sharing Fund of Chongqing University’s Large-scale Equipment,China
文摘The effects of the ultrasonic treatment on the microstructure and mechanical properties of Mg-6Zn-0.5Y-2Sn alloy were investigated. The results show that the ultrasonic treatment has significant effect on the microstructure and mechanical properties of Mg-6Zn-0.5Y-2Sn alloy. The phases in Mg-6Zn-0.5Y-2Sn alloy are α-Mg, MgZn2, MgSnY, Mg2Sn, and a small amount of I-phase. With the application of ultrasonic treatment, I-phase nearly disappears, and with increasing the ultrasonic treatment power, the coarse dendrites gradually change into roundish equiaxed grains. The second phases at the α-Mg boundaries transform from coarse, semicontinuous and non-uniform to fine, discontinuous, uniform and dispersive. When the ultrasonic treatment power is 700 W, the best comprehensive mechanical properties of Mg-6Zn-0.5Y-2Sn alloy are obtained. Compared with the untreated alloy, the 0.2%tensile yield strength, ultimate tensile strength and elongation are improved by 28%, 30%and 67%, respectively.
基金the Natural Science Foundation of Jiangsu Province of China(No.BK20160869)the financial support from the Nantong Science and Technology Project(No.GY12015009)+1 种基金the Fundamental Research Funds for the Central Universities(No.2015B01314)the National Natural Science Foundation of China(No.51501039).
文摘In this work,a high-strength Mg–10Gd–6Y–1.5Zn–0.5Zr(wt.%)alloy was fabricated by successive multi-pass equal channel angular pressing(ECAP).The microstructure and mechanical property of as-cast and ECAP alloys were systematically researched by X-ray diffractometer,scanning electron microscopy,transmission electron microscopy and compression test.The results show that the microstructure of as-cast alloy consists ofα-Mg grains,Mg24Y5 networks,18R blocks,fine 14H lamellas,and fewY-rich particles.After 8 passes ECAP,dynamic recrystallization ofα-Mg is developed and their average grain size decreases to about 1μm.The network Mg_(24)Y_(5) phase at grain boundaries is broken into small particles with average diameter lower than 0.5μm.Moreover,18R blocks are kinked and delaminated,or broken into small particles and blended with Mg24Y5 particles.14H lamellas grow gradually or are dynamically precipitated within certainα-Mg grains.Compression tests indicate that 8p ECAP alloy exhibits excellent mechanical property with compressive strength of 537 MPa and fracture strain of 17.0%.The significant improvement for both strength and ductility of deformed alloy could be ascribed to DRX grains,refined Mg24Y5 particles,18R kinking and dynamical precipitation of 14H.
基金Project(20921002)supported by the Innovative Research Groups of the National Natural Science Foundation of ChinaProject(21221061)supported by the National Natural Science Foundation of China+1 种基金Project(201105007)supported by the Science and Technology Program of Jilin Province,ChinaProject(20140325003GX)supported by the Science and Technology Support Project of Jilin Province,China
文摘Mg?1Zn?0.5Ca alloys were prepared by traditional steel mould casting and water-cooled copper mould injection casting at higher cooling rate. Microstructure, mechanical properties and bio-corrosion resistance of two alloys were contrastively investigated. Grain size reduces remarkably and microstructure becomes homogenous when raising cooling rate. The bio-corrosion behaviour in 3.5% sodium chloride solution (3.5% NaCl) and Hank’s solution at 37°C was investigated using electrochemical polarization measurement and the results indicate that the alloy prepared at higher cooling rates has better corrosion resistance in both types of solution. Further mass loss immersion test in Hank’s solution reveals the same result. The reason of corrosion resistance improvement is that raising cooling rate brings about homogeneous microstructure, which leads to micro-galvanic corrosion alleviation. The tensile test results show that yield strength, ultimate tensile strength and elongation are improved by raising cooling rate and the improvement is mainly due to grain refinement.
基金National Great Theoretic Research Project(2013CB632200)International Cooperation Project(2010DFR50010)Chongqing Science & Technology Support Project(CSTC2013jcyjC60001)
