Directional solidification of Al-15% (mass fraction) Cu alloy was investigated by in situ and real time radiography which was performed by Shanghai synchrotron radiation facility (SSRF). The imaging results reveal...Directional solidification of Al-15% (mass fraction) Cu alloy was investigated by in situ and real time radiography which was performed by Shanghai synchrotron radiation facility (SSRF). The imaging results reveal that columnar to equiaxed transition (CET) is provoked by external thermal disturbance. The detaching and floating of fragments of dendrite arms are the prelude of the transition when the solute boundary layer in front of the solid-liquid interface is thin. And the dendrite triangular tip is the fracture sensitive zone. When the conditions are suitable, new dendrites can sprout and grow up. This kind of dendrite has no obvious stem and is named anaxial columnar dendrites.展开更多
从碳钢连铸坯实际凝固组织入手对典型枝晶二次枝晶间距(secondary dendrite arm spacing,SDAS)进行测量分析,并发现了铸坯表面向中心凝固过程中的SDAS突增现象。结合铸坯横断面二维温度场数值模型分析可知,柱状晶向等轴晶转变(columnar ...从碳钢连铸坯实际凝固组织入手对典型枝晶二次枝晶间距(secondary dendrite arm spacing,SDAS)进行测量分析,并发现了铸坯表面向中心凝固过程中的SDAS突增现象。结合铸坯横断面二维温度场数值模型分析可知,柱状晶向等轴晶转变(columnar to equiaxed transition,CET)的过程会影响铸坯内部的传热过程,这种影响最终以典型枝晶SDAS突增的形式体现出来。基于典型枝晶SDAS突增现象,确立了铸坯内部CET定量判定的新方法,即将典型枝晶SDAS最大增加率的起始位置确定为铸坯内部CET起始位置。计算所得CET位置与铸坯内部温度梯度变化拐点的最大相对误差仅为8.3%,且与生长速率变化区间相对应,同时也与实际凝固组织形貌转变位置吻合,证明了该方法的有效性。展开更多
基金Natural Science Foundation of China(Nos.51790481,51790483,52130110,51901182)Natural Science Foundation of Shaanxi Province,China(No.2020JQ-157)Research Fund of the State Key Laboratory of Solidification Processing,China(No.2022-TS-01)。
基金Project(51001074)supported by the National Natural Science Foundation of ChinaProject(12ZR1414500)supported by Shanghai Municipal Natural Science Fund of ChinaProject(2012CB619505)supported by the National Basic Research Program of China
文摘Directional solidification of Al-15% (mass fraction) Cu alloy was investigated by in situ and real time radiography which was performed by Shanghai synchrotron radiation facility (SSRF). The imaging results reveal that columnar to equiaxed transition (CET) is provoked by external thermal disturbance. The detaching and floating of fragments of dendrite arms are the prelude of the transition when the solute boundary layer in front of the solid-liquid interface is thin. And the dendrite triangular tip is the fracture sensitive zone. When the conditions are suitable, new dendrites can sprout and grow up. This kind of dendrite has no obvious stem and is named anaxial columnar dendrites.
文摘从碳钢连铸坯实际凝固组织入手对典型枝晶二次枝晶间距(secondary dendrite arm spacing,SDAS)进行测量分析,并发现了铸坯表面向中心凝固过程中的SDAS突增现象。结合铸坯横断面二维温度场数值模型分析可知,柱状晶向等轴晶转变(columnar to equiaxed transition,CET)的过程会影响铸坯内部的传热过程,这种影响最终以典型枝晶SDAS突增的形式体现出来。基于典型枝晶SDAS突增现象,确立了铸坯内部CET定量判定的新方法,即将典型枝晶SDAS最大增加率的起始位置确定为铸坯内部CET起始位置。计算所得CET位置与铸坯内部温度梯度变化拐点的最大相对误差仅为8.3%,且与生长速率变化区间相对应,同时也与实际凝固组织形貌转变位置吻合,证明了该方法的有效性。